Information card for entry 7224299

Structure parameters

• Formula: C54 H82 B Ge N5
• Calculated formula: C48 H68 B Ge N5
• SMILES: [Ge]12(N(c3c(C(C)C)cccc3C(C)C)C=CN1c1c(C(C)C)cccc1C(C)C)N(c1c(C)cccc1C)B(N2c1c(cccc1C)C)N(C(C)C)C(C)C
• Title of publication: Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand
• Authors of publication: Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; Růžička, Aleš; Dostál, Libor
• Journal of publication: RSC Adv.
• Year of publication: 2016
• Journal volume: 6
• Journal issue: 23
• Pages of publication: 19377
• a: 12.41 ± 0.0012 Å
• b: 15.971 ± 0.0005 Å
• c: 26.276 ± 0.003 Å
• α: 101.799 ± 0.006°
• β: 95.207 ± 0.008°
• γ: 98.138 ± 0.005°
• Cell volume: 5007.9 ± 0.8 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0658
• Residual factor for significantly intense reflections: 0.0449
• Weighted residual factors for significantly intense reflections: 0.102
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No