Information card for entry 7224303

Structure parameters

• Formula: C22 H32 B Ge I2 N3
• Calculated formula: C22 H32 B Ge I2 N3
• SMILES: I[Ge]1(I)N(c2c(cccc2C)C)B(N1c1c(cccc1C)C)N(C(C)C)C(C)C
• Title of publication: Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand
• Authors of publication: Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; Růžička, Aleš; Dostál, Libor
• Journal of publication: RSC Adv.
• Year of publication: 2016
• Journal volume: 6
• Journal issue: 23
• Pages of publication: 19377
• a: 14.72 ± 0.0009 Å
• b: 8.214 ± 0.0007 Å
• c: 21.3591 ± 0.0015 Å
• α: 90°
• β: 94.762 ± 0.007°
• γ: 90°
• Cell volume: 2573.6 ± 0.3 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0615
• Weighted residual factors for all reflections included in the refinement: 0.0663
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No