Information card for entry 7224305

Structure parameters

• Formula: C40 H50 B Ge N3
• Calculated formula: C40 H50 B Ge N3
• SMILES: [Ge]12(N(c3c(C)cccc3C)B(N1c1c(cccc1C)C)N(C(C)C)C(C)C)CC(=C(C2)Cc1ccccc1)Cc1ccccc1
• Title of publication: Synthesis and reactivity of a germylene stabilized by a boraguanidinate ligand
• Authors of publication: Böserle, Jiří; Alonso, Mercedes; Jambor, Roman; Růžička, Aleš; Dostál, Libor
• Journal of publication: RSC Adv.
• Year of publication: 2016
• Journal volume: 6
• Journal issue: 23
• Pages of publication: 19377
• a: 13.726 ± 0.0007 Å
• b: 19.8081 ± 0.0017 Å
• c: 14.794 ± 0.0008 Å
• α: 90°
• β: 117.858 ± 0.004°
• γ: 90°
• Cell volume: 3556.1 ± 0.4 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0663
• Weighted residual factors for all reflections included in the refinement: 0.075
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No