Crystallography Open Database

Information card for entry 7225009

Preview

Coordinates	7225009.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H52 N51 O89 Si2 W24 Zn12.5
Calculated formula	C34 H35 N51 O89 Si2 W24 Zn12.5
Title of publication	Assembly of two novel 3D organic‒inorganic hybrids based on Keggin-type polyoxometalates: syntheses, crystal structures and properties
Authors of publication	Zhou, En-Long; Qin, Chao; Wang, Xin-Long; Shao, Kui-Zhan; Su, Zhong-Min
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	34
Pages of publication	6370
a	26.559 ± 0.0016 Å
b	27.6534 ± 0.0016 Å
c	21.9738 ± 0.0012 Å
α	90°
β	120.836 ± 0.001°
γ	90°
Cell volume	13857.2 ± 1.4 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	7
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.0874
Residual factor for significantly intense reflections	0.0547
Weighted residual factors for significantly intense reflections	0.1268
Weighted residual factors for all reflections included in the refinement	0.1462
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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