Information card for entry 7225508

Structure parameters

• Formula: C7 H14 Cl5 Ge2 N4
• Calculated formula: C7 H14 Cl5 Ge2 N4
• SMILES: [Ge]1(Cl)(Cl)N([Ge](Cl)(Cl)Cl)C(N(C)C)=CC(=[NH]1)N(C)C
• Title of publication: Synthesis, mechanism and ethylene polymerization catalysis of Ge(IV), Sn(II) and Zr(IV) complexes derived from substituted β-diketiminates
• Authors of publication: Xiao, Xia; Hao, Xiaomin; Bai, Jianliang; Chao, Jianbin; Cao, Wei; Chen, Xia
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 8.7293 ± 0.0016 Å
• b: 9.6018 ± 0.0018 Å
• c: 10.0436 ± 0.0019 Å
• α: 91.651 ± 0.002°
• β: 98.999 ± 0.002°
• γ: 102.452 ± 0.002°
• Cell volume: 810.2 ± 0.3 ų
• Cell temperature: 456 ± 2 K
• Ambient diffraction temperature: 456 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0335
• Weighted residual factors for significantly intense reflections: 0.0808
• Weighted residual factors for all reflections included in the refinement: 0.0831
• Goodness-of-fit parameter for all reflections included in the refinement: 1.015
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No