Information card for entry 7226779

Structure parameters

• Common name: [Os(H)(CO)(bpy)(tpp)2]+.PF6-.C7 H8
• Formula: C54 H47 F6 N2 O Os P6
• Calculated formula: C54 H46.5 F6 N2 O Os P3
• Title of publication: Heteroleptic [Os(H)(CO)(N(∧)N)(tpp)2](+) and [Os(Cl)(CO)(N(∧)N)(tpp)2](+) complexes - comparative studies of their luminescence properties.
• Authors of publication: Kamecka, Anna; Suwińska, Kinga; Kapturkiewicz, Andrzej
• Journal of publication: Physical chemistry chemical physics : PCCP
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 41
• Pages of publication: 28982 - 28996
• a: 14.649 ± 0.0007 Å
• b: 14.7296 ± 0.0007 Å
• c: 23.2685 ± 0.0012 Å
• α: 103.447 ± 0.001°
• β: 96.362 ± 0.002°
• γ: 91.092 ± 0.002°
• Cell volume: 4847.8 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0558
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for significantly intense reflections: 0.0859
• Weighted residual factors for all reflections included in the refinement: 0.0886
• Goodness-of-fit parameter for all reflections included in the refinement: 1.286
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No