Information card for entry 7227019

Structure parameters

• Formula: C14 H92 Mn7.5 N2 O106 Sb2 W18.5
• Calculated formula: C14 H24 Mn7.5 N2 O106 Sb2 W18.5
• Title of publication: Synthesis and characterization of a series of novel polyoxometalate-supported carbonyl manganese derivatives
• Authors of publication: Jia, Jiage; Zhang, Yanhui; Zhang, Panpan; Ma, Pengtao; Zhang, Dongdi; Wang, Jingping; Niu, Jingyang
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 12.581 ± 0.0019 Å
• b: 13.282 ± 0.002 Å
• c: 19.926 ± 0.003 Å
• α: 77.307 ± 0.002°
• β: 86.633 ± 0.002°
• γ: 63.697 ± 0.002°
• Cell volume: 2909.1 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0505
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0977
• Weighted residual factors for all reflections included in the refinement: 0.1028
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No