Information card for entry 7228054

Structure parameters

• Formula: C9 H5 O6 Yb
• Calculated formula: C9 H5 O6 Yb
• Title of publication: Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation
• Authors of publication: Breeze, Matthew I.; Chamberlain, Thomas W.; Clarkson, Guy J.; de Camargo, Raíssa Pires; Wu, Yue; de Lima, Juliana Fonseca; Millange, Franck; Serra, Osvaldo A.; O'Hare, Dermot; Walton, Richard I.
• Journal of publication: CrystEngComm
• Year of publication: 2017
• Journal volume: 19
• Journal issue: 17
• Pages of publication: 2424
• a: 10.56825 ± 0.00017 Å
• b: 12.66272 ± 0.00019 Å
• c: 6.6229 ± 0.00013 Å
• α: 90°
• β: 95.2274 ± 0.0017°
• γ: 90°
• Cell volume: 882.61 ± 0.03 ų
• Cell temperature: 296 ± 3 K
• Ambient diffraction temperature: 296 ± 3 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0627
• Residual factor for significantly intense reflections: 0.0561
• Weighted residual factors for significantly intense reflections: 0.1522
• Weighted residual factors for all reflections included in the refinement: 0.1554
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No