Information card for entry 7228056

Structure parameters

• Formula: C21 H20 N O9 Yb
• Calculated formula: C21 H20 N O9 Yb
• Title of publication: Structural variety in ytterbium dicarboxylate frameworks and in situ study diffraction of their solvothermal crystallisation
• Authors of publication: Breeze, Matthew I.; Chamberlain, Thomas W.; Clarkson, Guy J.; de Camargo, Raíssa Pires; Wu, Yue; de Lima, Juliana Fonseca; Millange, Franck; Serra, Osvaldo A.; O'Hare, Dermot; Walton, Richard I.
• Journal of publication: CrystEngComm
• Year of publication: 2017
• Journal volume: 19
• Journal issue: 17
• Pages of publication: 2424
• a: 8.4515 ± 0.0002 Å
• b: 12.3972 ± 0.0004 Å
• c: 12.568 ± 0.0003 Å
• α: 110.453 ± 0.002°
• β: 102.132 ± 0.002°
• γ: 109.619 ± 0.003°
• Cell volume: 1079.2 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.1032
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No