Information card for entry 7228329

Structure parameters

• Formula: C30 H65 N3 Ni O6 S2 Si2
• Calculated formula: C30 H65 N3 Ni O6 S2 Si2
• Title of publication: Structural, spectral and magnetic properties of Ni(II), Co(II) and Cd(II) compounds with imidazole derivatives and silanethiolate ligands
• Authors of publication: Kowalkowska, Daria; Dołęga, Anna; Nedelko, Natalia; Hnatejko, Zbigniew; Ponikiewski, Łukasz; Matracka, Alicja; Ślawska-Waniewska, Anna; Strągowska, Alicja; Słowy, Klaudia; Gazda, Maria; Pladzyk, Agnieszka
• Journal of publication: CrystEngComm
• Year of publication: 2017
• a: 14.3711 ± 0.0016 Å
• b: 32.952 ± 0.005 Å
• c: 9.537 ± 0.0011 Å
• α: 90°
• β: 103.618 ± 0.009°
• γ: 90°
• Cell volume: 4389.3 ± 1 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0834
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.1492
• Weighted residual factors for all reflections included in the refinement: 0.2048
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No