Information card for entry 7228335

Structure parameters

• Formula: C81 H136 La Li N2 O6 Si2
• Calculated formula: C77 H128 La1.0046 Li N2 O5 Si2
• Title of publication: Rigid NON-donor pincer ligand complexes of lutetium and lanthanum: synthesis and hydroamination catalysis
• Authors of publication: Motolko, Kelly S. A.; Emslie, David J. H.; Britten, James F.
• Journal of publication: RSC Adv.
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 45
• Pages of publication: 27938
• a: 16.931 ± 0.002 Å
• b: 23.782 ± 0.003 Å
• c: 21.09 ± 0.003 Å
• α: 90°
• β: 98.98 ± 0.003°
• γ: 90°
• Cell volume: 8387.9 ± 1.9 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1057
• Residual factor for significantly intense reflections: 0.084
• Weighted residual factors for significantly intense reflections: 0.2367
• Weighted residual factors for all reflections included in the refinement: 0.257
• Goodness-of-fit parameter for all reflections included in the refinement: 1.108
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No