Information card for entry 7228698

Structure parameters

• Formula: C34 H30 Br4 Co3 N4 O14
• Calculated formula: C34 H30 Br4 Co3 N4 O14
• Title of publication: Syntheses, crystal structures and catalytic activities of two solvent-induced homotrinuclear Co(ii) complexes with a naphthalenediol-based bis(Salamo)-type tetraoxime ligand
• Authors of publication: Li, Xiao-Yan; Chen, Le; Gao, Lei; Zhang, Yang; Akogun, Sunday Folaranmi; Dong, Wen-Kui
• Journal of publication: RSC Adv.
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 57
• Pages of publication: 35905
• a: 19.182 ± 0.002 Å
• b: 18.751 ± 0.002 Å
• c: 18.722 ± 0.002 Å
• α: 90°
• β: 113.614 ± 0.0018°
• γ: 90°
• Cell volume: 6170.1 ± 1.1 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296.15 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0794
• Residual factor for significantly intense reflections: 0.0511
• Weighted residual factors for significantly intense reflections: 0.1399
• Weighted residual factors for all reflections included in the refinement: 0.1496
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No