Reaction of sterically encumbered phenols, TEMPO-H, and organocarbonyl insertion reactions with L-AlH2 (L = HC(MeCNDipp)2, Dipp = 2,6-diisopropylphenyl)
Authors of publication
Keyes, Lauren K.; Todd, Angela D. K.; Giffin, Nick A.; Veinot, Alex J.; Hendsbee, Arthur D.; Robertson, Katherine N.; Geier, Stephen J.; Masuda, Jason D.
Journal of publication
RSC Adv.
Year of publication
2017
Journal volume
7
Journal issue
59
Pages of publication
37315
a
12.5098 ± 0.0016 Å
b
15.1447 ± 0.0019 Å
c
22.23 ± 0.003 Å
α
90°
β
104.731 ± 0.002°
γ
90°
Cell volume
4073.2 ± 0.9 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
99.97 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0847
Residual factor for significantly intense reflections
0.057
Weighted residual factors for significantly intense reflections
0.1379
Weighted residual factors for all reflections included in the refinement
0.1537
Goodness-of-fit parameter for all reflections included in the refinement
