Information card for entry 7229572

Structure parameters

• Common name: [[Pt(ppy)(biguH)]:(barbitone)].CHCl3
• Formula: C34 H35 Cl3 N8 O3 Pt
• Calculated formula: C34 H35 Cl3 N8 O3 Pt
• Title of publication: Cyclometallated Platinum(II) and Palladium(II) Complexes Containing 1,5-Diarylbiguanides: Synthesis, Characterisation and Hydrogen Bond-directed Assembly
• Authors of publication: McMorran, David; McKay, Aidan P.; Gordon, Keith; Shillito, Georgina E.
• Journal of publication: CrystEngComm
• Year of publication: 2017
• a: 13.6217 ± 0.0004 Å
• b: 33.0468 ± 0.0009 Å
• c: 7.813 ± 0.0002 Å
• α: 90°
• β: 99.978 ± 0.003°
• γ: 90°
• Cell volume: 3463.85 ± 0.17 ų
• Cell temperature: 100 ± 0.01 K
• Ambient diffraction temperature: 100 ± 0.01 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.045
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for significantly intense reflections: 0.0899
• Weighted residual factors for all reflections included in the refinement: 0.0957
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No