Information card for entry 7230206

Structure parameters

• Common name: Metoclopramide hydrochloride oxalic acid
• Chemical name: 4-Amino-5-chloro-N-(2-(diethylamino)ethyl)-2-methoxybenzamide hydrochloride oxalic acid
• Formula: C15 H24 Cl2 N3 O4
• Calculated formula: C15 H24 Cl2 N3 O4
• Title of publication: Suppressed hydration in metoclopramide hydrochloride by salt cocrystallisation
• Authors of publication: Nugraha, Yuda Prasetya; Uekusa, Hidehiro
• Journal of publication: CrystEngComm
• Year of publication: 2018
• Journal volume: 20
• Journal issue: 19
• Pages of publication: 2653
• a: 7.527 ± 0.0004 Å
• b: 14.1483 ± 0.0009 Å
• c: 34.3682 ± 0.0019 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3660 ± 0.4 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0488
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0875
• Weighted residual factors for all reflections included in the refinement: 0.0928
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No