Crystallography Open Database

Information card for entry 7230273

Preview

Coordinates	7230273.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H416 Cl25 Co7 Gd45 O388
Calculated formula	C81 H168 Cl4 Co7 Gd45 O254
Title of publication	Four 3d‒4f heterometallic Ln45M7 clusters protected by mixed ligands
Authors of publication	Fan, Shen; Xu, Su-Hui; Zheng, Xiu-Ying; Yan, Zhi-Hao; Kong, Xiang-Jian; Long, La-Sheng; Zheng, Lan-Sun
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	15
Pages of publication	2120
a	31.5773 ± 0.0005 Å
b	36.4648 ± 0.0005 Å
c	38.7297 ± 0.0009 Å
α	90°
β	107.41 ± 0.002°
γ	90°
Cell volume	42552.7 ± 1.4 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1308
Residual factor for significantly intense reflections	0.0835
Weighted residual factors for significantly intense reflections	0.22
Weighted residual factors for all reflections included in the refinement	0.2517
Goodness-of-fit parameter for all reflections included in the refinement	1.031
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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