Crystallography Open Database

Information card for entry 7230276

Preview

Coordinates	7230276.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C82 H416 Cl25 Dy45 Ni7 O388
Calculated formula	C82 H176 Cl4 Dy45 Ni7 O253
Title of publication	Four 3d‒4f heterometallic Ln45M7 clusters protected by mixed ligands
Authors of publication	Fan, Shen; Xu, Su-Hui; Zheng, Xiu-Ying; Yan, Zhi-Hao; Kong, Xiang-Jian; Long, La-Sheng; Zheng, Lan-Sun
Journal of publication	CrystEngComm
Year of publication	2018
Journal volume	20
Journal issue	15
Pages of publication	2120
a	31.3304 ± 0.0013 Å
b	35.9748 ± 0.001 Å
c	39.1007 ± 0.0015 Å
α	90°
β	107.174 ± 0.004°
γ	90°
Cell volume	42106 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1762
Residual factor for significantly intense reflections	0.1043
Weighted residual factors for significantly intense reflections	0.2529
Weighted residual factors for all reflections included in the refinement	0.3065
Goodness-of-fit parameter for all reflections included in the refinement	0.971
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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