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Information card for entry 7230470
Preview
Coordinates | 7230470.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | bis(2-benzyl-3,5-diphenyl-2,3-dihydro-1H-pyrazol-1-yl)palladium(IV) chloride |
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Formula | C22 H18 Cl N2 Pd0.5 |
Calculated formula | C22 H18 Cl N2 Pd0.5 |
Title of publication | Synthesis, characterization and evaluation of bulky bis(pyrazolyl)palladium complexes in Suzuki‒Miyaura cross-coupling reactions |
Authors of publication | Ocansey, Edward; Darkwa, James; Makhubela, Banothile C. E. |
Journal of publication | RSC Advances |
Year of publication | 2018 |
Journal volume | 8 |
Journal issue | 25 |
Pages of publication | 13826 |
a | 6.7767 ± 0.0006 Å |
b | 10.2586 ± 0.0009 Å |
c | 13.5319 ± 0.0013 Å |
α | 102.123 ± 0.002° |
β | 98.442 ± 0.002° |
γ | 94.97 ± 0.002° |
Cell volume | 903.05 ± 0.14 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0316 |
Residual factor for significantly intense reflections | 0.0287 |
Weighted residual factors for significantly intense reflections | 0.0674 |
Weighted residual factors for all reflections included in the refinement | 0.0687 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.082 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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