Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7230562
Preview
Coordinates | 7230562.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C31 H25 Cl2 N O2 |
---|---|
Calculated formula | C31 H25 Cl2 N O2 |
Title of publication | Diastereoselective construction of 4-indole substituted chromans bearing a ketal motif through a three-component Friedel‒Crafts alkylation/ketalization sequence |
Authors of publication | Guo, Jiao-Mei; Wang, Wen-Bo; Guo, Jia; Zhu, Yan-Shuo; Bai, Xu-Guan; Jin, Shao-Jing; Wang, Qi-Lin; Bu, Zhan-Wei |
Journal of publication | RSC Advances |
Year of publication | 2018 |
Journal volume | 8 |
Journal issue | 28 |
Pages of publication | 15641 |
a | 9.3851 ± 0.0006 Å |
b | 11.5543 ± 0.0008 Å |
c | 12.0921 ± 0.0008 Å |
α | 95.088 ± 0.001° |
β | 91.155 ± 0.001° |
γ | 104.026 ± 0.001° |
Cell volume | 1265.96 ± 0.15 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0513 |
Residual factor for significantly intense reflections | 0.0375 |
Weighted residual factors for significantly intense reflections | 0.0992 |
Weighted residual factors for all reflections included in the refinement | 0.107 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.034 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7230562.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.