A chiral spiroborate anion from diphenyl-l-tartramide [B{l-Tar(NHPh)2}2]−applied to some challenging resolutions
Authors of publication
Wong, Lawrence W.-Y.; Tam, Gemma S.-S.; Chen, Xiaoyan; So, Frederick T.-K.; Soecipto, Aristyo; Sheong, Fu Kit; Sung, Herman H.-Y.; Lin, Zhenyang; Williams, Ian D.
Journal of publication
CrystEngComm
Year of publication
2018
Journal volume
20
Journal issue
33
Pages of publication
4831
a
28.62 ± 0.0011 Å
b
5.25819 ± 0.00014 Å
c
28.609 ± 0.0009 Å
α
90°
β
113.834 ± 0.004°
γ
90°
Cell volume
3938.2 ± 0.3 Å3
Cell temperature
100 ± 0.1 K
Ambient diffraction temperature
100 ± 0.1 K
Number of distinct elements
5
Space group number
5
Hermann-Mauguin space group symbol
C 1 2 1
Hall space group symbol
C 2y
Residual factor for all reflections
0.0396
Residual factor for significantly intense reflections
0.0364
Weighted residual factors for significantly intense reflections
0.095
Weighted residual factors for all reflections included in the refinement
0.0972
Goodness-of-fit parameter for all reflections included in the refinement
