Information card for entry 7231627

Structure parameters

• Formula: C30 H22 Cl0.75 N O3
• Calculated formula: C30 H22 Cl0.757 N O3
• Title of publication: Advanced palladium free approach to the synthesis of substituted alkene oxindoles via aluminum-promoted Knoevenagel reaction
• Authors of publication: Novikova, Daria S.; Grigoreva, Tatyana A.; Zolotarev, Andrey A.; Garabadzhiu, Alexander V.; Tribulovich, Vyacheslav G.
• Journal of publication: RSC Advances
• Year of publication: 2018
• Journal volume: 8
• Journal issue: 60
• Pages of publication: 34543
• a: 10.226 ± 0.0007 Å
• b: 10.6156 ± 0.0008 Å
• c: 11.7663 ± 0.0008 Å
• α: 69.018 ± 0.007°
• β: 85.368 ± 0.006°
• γ: 85.951 ± 0.006°
• Cell volume: 1187.51 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1133
• Weighted residual factors for all reflections included in the refinement: 0.1196
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No