Information card for entry 7231700

Structure parameters

• Formula: C88 H76 Cl8 N4 Ni2 O6
• Calculated formula: C88 H76 Cl8 N4 Ni2 O6
• Title of publication: Bis-(salicylaldehyde-benzhydrylimino)nickel complexes with different electron groups: crystal structure and their catalytic properties toward (co)polymerization of norbornene and 1-hexene
• Authors of publication: He, Xiaohui; Tu, Guangshui; Zhang, Feng; Huang, Shengmei; Cheng, Changwen; Zhu, Chuanyi; Duan, Yapeng; Wang, Suli; Chen, Defu
• Journal of publication: RSC Advances
• Year of publication: 2018
• Journal volume: 8
• Journal issue: 63
• Pages of publication: 36298
• a: 9.1018 ± 0.001 Å
• b: 13.8097 ± 0.0015 Å
• c: 16.5217 ± 0.0017 Å
• α: 73.923 ± 0.002°
• β: 74.397 ± 0.001°
• γ: 81.837 ± 0.002°
• Cell volume: 1916.8 ± 0.4 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1887
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for significantly intense reflections: 0.0762
• Weighted residual factors for all reflections included in the refinement: 0.0905
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No