Information card for entry 7232523

Structure parameters

• Formula: C7 H32 B18 Co N
• Calculated formula: C7 H32 B18 Co N
• Title of publication: 3,2,1 and stop! An innovative, straightforward and clean route for the flash synthesis of metallacarboranes
• Authors of publication: Bennour, Ines; Cioran, Ana M.; Teixidor, Francesc; Viñas, Clara
• Journal of publication: Green Chemistry
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 8
• Pages of publication: 1925
• a: 9.13 ± 0.011 Å
• b: 10.446 ± 0.01 Å
• c: 11.101 ± 0.009 Å
• α: 90°
• β: 106.63 ± 0.04°
• γ: 90°
• Cell volume: 1014.4 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0694
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.1723
• Weighted residual factors for all reflections included in the refinement: 0.1741
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No