Information card for entry 7232640

Structure parameters

• Formula: C30 H40 I4 N8 Ni2 O2
• Calculated formula: C30 H40 I4 N8 Ni2 O2
• Title of publication: Solvent-Free Synthesis and Reactivity of Nickel(II) Borohydride and Nickel(II) Hydride
• Authors of publication: Angamuthu, Raja; Raje, Sakthi
• Journal of publication: Green Chemistry
• Year of publication: 2019
• a: 19.061 ± 0.004 Å
• b: 10.993 ± 0.002 Å
• c: 19.32 ± 0.004 Å
• α: 90°
• β: 112.098 ± 0.005°
• γ: 90°
• Cell volume: 3750.9 ± 1.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1494
• Residual factor for significantly intense reflections: 0.1157
• Weighted residual factors for significantly intense reflections: 0.3284
• Weighted residual factors for all reflections included in the refinement: 0.37
• Goodness-of-fit parameter for all reflections included in the refinement: 1.459
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No