Information card for entry 7232707

Structure parameters

• Formula: C32 H16 Ce4 Cl Cr4 Cs2 O83.5 Si W12
• Calculated formula: C32 H16 Ce4 Cl Cr4 Cs2 O83.5 Si W12
• Title of publication: Incorporating polyoxometalates and organic ligands to pursue 3d‒4f heterometallic clusters: a series of {Cr4Ln4} clusters stabilized by phthalic acid and [SiW12O40]4−
• Authors of publication: Gu, Ya-Nan; Zhao, Dan; Yu, Hao; Ge, Rui; Li, Zhong; Tian, Chong-Bian; Li, Xin-Xiong; Sun, Yan-Qiong; Zheng, Shou-Tian
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 24
• Pages of publication: 13543
• a: 13.5174 ± 0.0011 Å
• b: 13.5216 ± 0.0011 Å
• c: 29.869 ± 0.002 Å
• α: 81.6102 ± 0.0015°
• β: 82.6279 ± 0.0016°
• γ: 89.5941 ± 0.0017°
• Cell volume: 5355.9 ± 0.7 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0751
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for significantly intense reflections: 0.1818
• Weighted residual factors for all reflections included in the refinement: 0.1897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No