Crystallography Open Database

Information card for entry 7232946

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Coordinates	7232946.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H64 N8 Ni6 O25
Calculated formula	C56 H64 N8 Ni6 O25
Title of publication	Variation of nuclearity in NiII complexes of a Schiff base ligand: crystal structures and magnetic studies
Authors of publication	Ghosh, Tanmoy Kumar; Mahapatra, Prithwish; Jana, Subrata; Ghosh, Ashutosh
Journal of publication	CrystEngComm
Year of publication	2019
Journal volume	21
Journal issue	31
Pages of publication	4620
a	20.212 ± 0.011 Å
b	22.656 ± 0.011 Å
c	16.048 ± 0.008 Å
α	90°
β	121.342 ± 0.01°
γ	90°
Cell volume	6276 ± 6 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1349
Residual factor for significantly intense reflections	0.0617
Weighted residual factors for significantly intense reflections	0.1596
Weighted residual factors for all reflections included in the refinement	0.2121
Goodness-of-fit parameter for all reflections included in the refinement	1.008
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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