Information card for entry 7232948

Structure parameters

• Formula: C32 H44 N8 Ni2 O13
• Calculated formula: C32 H44 N8 Ni2 O13
• Title of publication: Variation of nuclearity in NiII complexes of a Schiff base ligand: crystal structures and magnetic studies
• Authors of publication: Ghosh, Tanmoy Kumar; Mahapatra, Prithwish; Jana, Subrata; Ghosh, Ashutosh
• Journal of publication: CrystEngComm
• Year of publication: 2019
• Journal volume: 21
• Journal issue: 31
• Pages of publication: 4620
• a: 22.233 ± 0.004 Å
• b: 7.3217 ± 0.0014 Å
• c: 23.045 ± 0.004 Å
• α: 90°
• β: 101.296 ± 0.004°
• γ: 90°
• Cell volume: 3678.7 ± 1.2 ų
• Cell temperature: 299 ± 2 K
• Ambient diffraction temperature: 299 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0448
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0947
• Weighted residual factors for all reflections included in the refinement: 0.099
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No