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Information card for entry 7233391
Preview
Coordinates | 7233391.cif |
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Original paper (by DOI) | HTML |
Chemical name | Diethyl-(1-((1-((tert-butyldimethylsilyl)oxy)-2-methylpropan-2-yl) (1-(pyridin-2-yl)ethoxy)amino)-2,2-dimethylpropyl)phosphonate-k2NPy,OP=O- bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato-k2O,O')zinc(II)] |
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Formula | C36 H53 F12 N2 O9 P Si Zn |
Calculated formula | C36 H53 F12 N2 O9 P Si Zn |
Title of publication | How intramolecular coordination bonding (ICB) controls the homolysis of the C‒ON bond in alkoxyamines |
Authors of publication | Audran, Gérard; Bagryanskaya, Elena; Bagryanskaya, Irina; Edeleva, Mariya; Joly, Jean-Patrick; Marque, Sylvain R. A.; Iurchenkova, Anna; Kaletina, Polina; Cherkasov, Sergey; Hai, Tung To; Tretyakov, Evgeny; Zhivetyeva, Svetlana |
Journal of publication | RSC Advances |
Year of publication | 2019 |
Journal volume | 9 |
Journal issue | 44 |
Pages of publication | 25776 |
a | 11.3993 ± 0.0006 Å |
b | 13.6801 ± 0.0008 Å |
c | 16.1856 ± 0.0009 Å |
α | 96.668 ± 0.002° |
β | 94.471 ± 0.002° |
γ | 100.497 ± 0.002° |
Cell volume | 2452.3 ± 0.2 Å3 |
Cell temperature | 296 ± 2 K |
Ambient diffraction temperature | 296 ± 2 K |
Number of distinct elements | 8 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0686 |
Residual factor for significantly intense reflections | 0.0448 |
Weighted residual factors for significantly intense reflections | 0.1255 |
Weighted residual factors for all reflections included in the refinement | 0.1784 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7233391.html
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Users of the data should acknowledge the original authors of the
structural data.