Crystallography Open Database

Information card for entry 7233593

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Coordinates	7233593.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H40 O6 P2
Calculated formula	C36 H40 O6 P2
Title of publication	Catalyst-free hydrophosphination of alkenes in presence of 2-methyltetrahydrofuran: a green and easy access to a wide range of tertiary phosphines
Authors of publication	Bissessar, Damien; Egly, Julien; Achard, Thierry; Steffanut, Pascal; Bellemin-Laponnaz, Stéphane
Journal of publication	RSC Advances
Year of publication	2019
Journal volume	9
Journal issue	47
Pages of publication	27250
a	5.6788 ± 0.0004 Å
b	8.9086 ± 0.0004 Å
c	16.4624 ± 0.0011 Å
α	90.613 ± 0.004°
β	92.777 ± 0.003°
γ	103.471 ± 0.003°
Cell volume	808.76 ± 0.09 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.2133
Residual factor for significantly intense reflections	0.1689
Weighted residual factors for significantly intense reflections	0.4599
Weighted residual factors for all reflections included in the refinement	0.4923
Goodness-of-fit parameter for all reflections included in the refinement	1.847
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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