Information card for entry 7234158

Structure parameters

• Formula: C17 H21 N O4
• Calculated formula: C17 H21 N O4
• Title of publication: Formal synthesis of (+)-lactacystin from l-serine
• Authors of publication: Bulman Page, Philip C.; Goodyear, Ross L.; Chan, Yohan; Slawin, Alexandra M. Z.; Allin, Steven M.
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 51
• Pages of publication: 30019
• a: 15.5906 ± 0.00016 Å
• b: 5.83233 ± 0.00005 Å
• c: 19.3142 ± 0.0002 Å
• α: 90°
• β: 112.98 ± 0.0013°
• γ: 90°
• Cell volume: 1616.86 ± 0.03 ų
• Cell temperature: 125 K
• Ambient diffraction temperature: 125 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.1111
• Weighted residual factors for all reflections included in the refinement: 0.1119
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No