Crystallography Open Database

Information card for entry 7234160

Preview

Coordinates	7234160.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H27 N O5
Calculated formula	C24 H27 N O5
Title of publication	Formal synthesis of (+)-lactacystin from l-serine
Authors of publication	Bulman Page, Philip C.; Goodyear, Ross L.; Chan, Yohan; Slawin, Alexandra M. Z.; Allin, Steven M.
Journal of publication	RSC Advances
Year of publication	2019
Journal volume	9
Journal issue	51
Pages of publication	30019
a	6.24701 ± 0.00005 Å
b	17.7899 ± 0.00014 Å
c	20.2686 ± 0.00016 Å
α	90°
β	90°
γ	90°
Cell volume	2252.52 ± 0.03 Å³
Cell temperature	125 K
Ambient diffraction temperature	125 K
Number of distinct elements	4
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for all reflections	0.0459
Residual factor for significantly intense reflections	0.0454
Weighted residual factors for significantly intense reflections	0.1325
Weighted residual factors for all reflections included in the refinement	0.1331
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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