Information card for entry 7234985

Structure parameters

• Formula: C23 H21 N S
• Calculated formula: C23 H21 N S
• Title of publication: Ultra-small palladium nano-particles synthesized using bulky S/Se and N donor ligands as a stabilizer: application as catalysts for Suzuki‒Miyaura coupling
• Authors of publication: Oswal, Preeti; Arora, Aayushi; Kaushal, Jolly; Rao, Gyandshwar Kumar; Kumar, Sushil; Singh, Ajai K.; Kumar, Arun
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 39
• Pages of publication: 22313
• a: 5.3825 ± 0.0007 Å
• b: 15.3166 ± 0.0013 Å
• c: 21.472 ± 0.003 Å
• α: 89.91 ± 0.008°
• β: 84.752 ± 0.01°
• γ: 89.905 ± 0.009°
• Cell volume: 1762.8 ± 0.4 ų
• Cell temperature: 150.01 ± 0.1 K
• Ambient diffraction temperature: 150.01 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1042
• Residual factor for significantly intense reflections: 0.0821
• Weighted residual factors for significantly intense reflections: 0.2427
• Weighted residual factors for all reflections included in the refinement: 0.2912
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No