Information card for entry 7234996

Structure parameters

• Formula: C19 H8 N0.5 O12 U
• Calculated formula: C19 H8 N0.5 O12 U
• Title of publication: Time-controlled synthesis of the 3D coordination polymer U(1,2,3-Hbtc)2 followed by the formation of molecular poly-oxo cluster {U14} containing hemimellitate uranium(iv)
• Authors of publication: Dufaye, Maxime; Martin, Nicolas P.; Duval, Sylvain; Volkringer, Christophe; Ikeda-Ohno, Atsushi; Loiseau, Thierry
• Journal of publication: RSC Advances
• Year of publication: 2019
• Journal volume: 9
• Journal issue: 40
• Pages of publication: 22795
• a: 11.7099 ± 0.0016 Å
• b: 11.7099 ± 0.0016 Å
• c: 27.227 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3733.4 ± 0.9 ų
• Cell temperature: 299.92 K
• Ambient diffraction temperature: 299.92 K
• Number of distinct elements: 5
• Space group number: 88
• Hermann-Mauguin space group symbol: I 41/a :2
• Hall space group symbol: -I 4ad
• Residual factor for all reflections: 0.0407
• Residual factor for significantly intense reflections: 0.0208
• Weighted residual factors for significantly intense reflections: 0.0422
• Weighted residual factors for all reflections included in the refinement: 0.0471
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No