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Information card for entry 7235004
Preview
Coordinates | 7235004.cif |
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Original paper (by DOI) | HTML |
Chemical name | 2-(trimethylsilyl)ethyl-4-azido-3-O-benzyl-4,6-dideoxy-alpha-D-mannopyranosyl-(1->2)-4-azido-3-O-benzyl-4,6-dideoxy-alpha-D-mannopyranosyl-(1->2)-4-azido-3-O-benzyl-4,6-dideoxy-alpha-D-mannopyranoside |
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Formula | C44 H59 N9 O10 Si |
Calculated formula | C44 H59 N9 O10 Si |
Title of publication | Towards the complete synthetic O-antigen of Vibrio cholerae O1, serotype inaba: improved synthesis of the conjugation-ready upstream terminal hexasaccharide determinant |
Authors of publication | Mukherjee, Mana Mohan; Xu, Peng; Stevens, Edwin D.; Kováč, Pavol |
Journal of publication | RSC Advances |
Year of publication | 2019 |
Journal volume | 9 |
Journal issue | 62 |
Pages of publication | 36440 |
a | 11.53 ± 0.003 Å |
b | 16.862 ± 0.004 Å |
c | 25.697 ± 0.006 Å |
α | 90° |
β | 98.067 ± 0.004° |
γ | 90° |
Cell volume | 4947 ± 2 Å3 |
Cell temperature | 120 ± 2 K |
Ambient diffraction temperature | 120 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0691 |
Residual factor for significantly intense reflections | 0.0445 |
Weighted residual factors for significantly intense reflections | 0.1034 |
Weighted residual factors for all reflections included in the refinement | 0.1171 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.038 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7235004.html
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