Crystallography Open Database

Information card for entry 7235239

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Coordinates	7235239.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H33 N3 O3
Calculated formula	C30 H33 N3 O3
Title of publication	Allylation of isatin-derived N-Boc-hydrazones followed by Pd-catalyzed carboamination reaction: an entry to 3-spiro-pyrazolidyl-oxindoles
Authors of publication	Gazzotti, Stefano; Manenti, Marco; Lo Presti, Leonardo; Silvani, Alessandra
Journal of publication	RSC Advances
Year of publication	2019
Journal volume	9
Journal issue	65
Pages of publication	37788
a	10.6314 ± 0.0002 Å
b	24.1537 ± 0.0004 Å
c	10.5798 ± 0.0002 Å
α	90°
β	103.663 ± 0.001°
γ	90°
Cell volume	2639.88 ± 0.08 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0838
Residual factor for significantly intense reflections	0.0591
Weighted residual factors for significantly intense reflections	0.1819
Weighted residual factors for all reflections included in the refinement	0.2029
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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