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Information card for entry 7235274
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Coordinates | 7235274.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 17b |
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Chemical name | 17b |
Formula | C19 H14 O5 S4 |
Calculated formula | C19 H14 O5 S4 |
Title of publication | Straightforward access to aryl-substituted/fused 1,3-dithiole-2-chalcogenones by Cu-catalyzed C‒S coupling between aryl iodides and zinc‒thiolate complex (TBA)2[Zn(DMIT)2] |
Authors of publication | Sun, Jibin; Lu, Xiaofeng; Shao, Jiafeng; Cui, Zili; Shao, Yu; Jiang, Guiyang; Yu, Wei; Shao, Xiangfeng |
Journal of publication | RSC Advances |
Year of publication | 2013 |
Journal volume | 3 |
Journal issue | 26 |
Pages of publication | 10193 |
a | 12.696 ± 0.009 Å |
b | 17.151 ± 0.012 Å |
c | 10.238 ± 0.007 Å |
α | 90° |
β | 114.694 ± 0.005° |
γ | 90° |
Cell volume | 2025 ± 2 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for all reflections | 0.0718 |
Residual factor for significantly intense reflections | 0.0426 |
Weighted residual factors for significantly intense reflections | 0.0916 |
Weighted residual factors for all reflections included in the refinement | 0.1073 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.018 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7235274.html
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