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Information card for entry 7235276
Preview
Coordinates | 7235276.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | 34a |
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Chemical name | 34a |
Formula | C11 H6 O2 S5 |
Calculated formula | C11 H6 O2 S5 |
Title of publication | Straightforward access to aryl-substituted/fused 1,3-dithiole-2-chalcogenones by Cu-catalyzed C‒S coupling between aryl iodides and zinc‒thiolate complex (TBA)2[Zn(DMIT)2] |
Authors of publication | Sun, Jibin; Lu, Xiaofeng; Shao, Jiafeng; Cui, Zili; Shao, Yu; Jiang, Guiyang; Yu, Wei; Shao, Xiangfeng |
Journal of publication | RSC Advances |
Year of publication | 2013 |
Journal volume | 3 |
Journal issue | 26 |
Pages of publication | 10193 |
a | 10.892 ± 0.003 Å |
b | 8.013 ± 0.0019 Å |
c | 14.444 ± 0.003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1260.6 ± 0.5 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 4 |
Space group number | 62 |
Hermann-Mauguin space group symbol | P m n b |
Hall space group symbol | -P 2bc 2a |
Residual factor for all reflections | 0.0466 |
Residual factor for significantly intense reflections | 0.0346 |
Weighted residual factors for significantly intense reflections | 0.0814 |
Weighted residual factors for all reflections included in the refinement | 0.0919 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7235276.html
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