Crystallography Open Database

Information card for entry 7235343

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Coordinates	7235343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H18 Cl2 N2
Calculated formula	C22 H18 Cl2 N2
Title of publication	An efficient facile and one-pot synthesis of benzodiazepines and chemoselective 1,2-disubstituted benzimidazoles using a magnetically retrievable Fe3O4 nanocatalyst under solvent free conditions
Authors of publication	Jamatia, Ramen; Saha, Mithu; Pal, Amarta Kumar
Journal of publication	RSC Adv.
Year of publication	2014
Journal volume	4
Journal issue	25
Pages of publication	12826
a	14.0976 ± 0.0012 Å
b	10.017 ± 0.0007 Å
c	14.9301 ± 0.0013 Å
α	90°
β	116.746 ± 0.011°
γ	90°
Cell volume	1882.8 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0979
Residual factor for significantly intense reflections	0.0548
Weighted residual factors for significantly intense reflections	0.1174
Weighted residual factors for all reflections included in the refinement	0.1375
Goodness-of-fit parameter for all reflections included in the refinement	1.018
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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