Information card for entry 7235480

Structure parameters

• Formula: C20 H17.25 Br N O3
• Calculated formula: C20 H16 Br N O3
• Title of publication: Synthesis of benzo[a]carbazoles and indolo[2,3-a]carbazoles via photoinduced carbene-mediated C‒H insertion reaction
• Authors of publication: Yang, Jidong; Zhang, Qingzhao; Zhang, Wei; Yu, Wei
• Journal of publication: RSC Adv.
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 26
• Pages of publication: 13704
• a: 14.3664 ± 0.0006 Å
• b: 14.1501 ± 0.0006 Å
• c: 17.8928 ± 0.0008 Å
• α: 90°
• β: 112.334 ± 0.005°
• γ: 90°
• Cell volume: 3364.5 ± 0.3 ų
• Cell temperature: 293.1 ± 0.7 K
• Ambient diffraction temperature: 293.1 ± 0.7 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1232
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections included in the refinement: 0.0989
• Goodness-of-fit parameter for all reflections included in the refinement: 0.977
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No