Information card for entry 7235558

Structure parameters

• Formula: C12 H10 Br2 N4 Pb
• Calculated formula: C12 H10 Br2 N4 Pb
• Title of publication: Solid state structural transformation of bromide coordination polymer to chloride by anion replacement; new precursors for preparation of PbBr2 and PbCl2 nanoparticles
• Authors of publication: Hashemi, Lida; Morsali, Ali
• Journal of publication: RSC Adv.
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 33
• Pages of publication: 17265
• a: 4.1774 ± 0.0005 Å
• b: 9.2283 ± 0.0012 Å
• c: 10.8275 ± 0.0014 Å
• α: 108.661 ± 0.002°
• β: 95.978 ± 0.002°
• γ: 91.459 ± 0.002°
• Cell volume: 392.54 ± 0.09 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0139
• Residual factor for significantly intense reflections: 0.0139
• Weighted residual factors for significantly intense reflections: 0.0327
• Weighted residual factors for all reflections included in the refinement: 0.0327
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No