Information card for entry 7235717
| Formula |
C16 H12 Cl2 O4 |
| Calculated formula |
C16 H12 Cl2 O4 |
| Title of publication |
Metal-free DDQ-mediated oxidative C‒O coupling of acetalic sp3C‒H bonds with carboxylic acids |
| Authors of publication |
Li, Jiang-Sheng; Xue, Yuan; Fu, Dong-Mei; Li, Dao-Lin; Li, Zhi-Wei; Liu, Wei-Dong; Pang, Huai-Lin; Zhang, Yue-Fei; Cao, Zhong; Zhang, Ling |
| Journal of publication |
RSC Adv. |
| Year of publication |
2014 |
| Journal volume |
4 |
| Journal issue |
96 |
| Pages of publication |
54039 |
| a |
7.7369 ± 0.0015 Å |
| b |
7.9449 ± 0.0016 Å |
| c |
12.788 ± 0.003 Å |
| α |
104.35 ± 0.03° |
| β |
97.85 ± 0.03° |
| γ |
92.83 ± 0.03° |
| Cell volume |
751.6 ± 0.3 Å3 |
| Cell temperature |
173 ± 2 K |
| Ambient diffraction temperature |
173 ± 2 K |
| Number of distinct elements |
4 |
| Space group number |
2 |
| Hermann-Mauguin space group symbol |
P -1 |
| Hall space group symbol |
-P 1 |
| Residual factor for all reflections |
0.0764 |
| Residual factor for significantly intense reflections |
0.0445 |
| Weighted residual factors for significantly intense reflections |
0.0917 |
| Weighted residual factors for all reflections included in the refinement |
0.1075 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.01 |
| Diffraction radiation wavelength |
0.71073 Å |
| Diffraction radiation type |
MoKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/7235717.html
