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Information card for entry 7235725
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 7235725.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C19 H21 F5 N2 O S |
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Calculated formula | C19 H21 F5 N2 O S |
Title of publication | First efficient synthesis of SF5-substituted pyrrolidines using 1,3-dipolar cycloaddition of azomethine ylides with pentafluorosulfanyl-substituted acrylic esters and amides |
Authors of publication | Falkowska, Ewelina; Tognetti, Vincent; Joubert, Laurent; Jubault, Philippe; Bouillon, Jean-Philippe; Pannecoucke, Xavier |
Journal of publication | RSC Advances |
Year of publication | 2015 |
Journal volume | 5 |
Journal issue | 9 |
Pages of publication | 6864 |
a | 9.2994 ± 0.0009 Å |
b | 12.5496 ± 0.0012 Å |
c | 17.0351 ± 0.0016 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1988.1 ± 0.3 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n 21 a |
Hall space group symbol | P -2ac -2n |
Residual factor for all reflections | 0.0919 |
Residual factor for significantly intense reflections | 0.0555 |
Weighted residual factors for significantly intense reflections | 0.1212 |
Weighted residual factors for all reflections included in the refinement | 0.1393 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.952 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7235725.html
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Users of the data should acknowledge the original authors of the
structural data.