Information card for entry 7236102

Structure parameters

• Formula: C240 H288 N36 O90 Tb6
• Calculated formula: C231 H96 N39 O67 Tb6
• Title of publication: An unprecedented anionic Ln-MOF with a cage-within-cage motif: spontaneous reduction and immobilization of ion-exchanged Pd(ii) to Pd-NPs in the framework
• Authors of publication: Han, Yun-Hu; Tian, Chong-Bin; Lin, Ping; Du, Shao-Wu
• Journal of publication: Journal of Materials Chemistry A
• Year of publication: 2015
• Journal volume: 3
• Journal issue: 48
• Pages of publication: 24525
• a: 26.7264 ± 0.0013 Å
• b: 26.7264 ± 0.0013 Å
• c: 26.7264 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 19090.7 ± 1.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 204
• Hermann-Mauguin space group symbol: I m -3
• Hall space group symbol: -I 2 2 3
• Residual factor for all reflections: 0.0715
• Residual factor for significantly intense reflections: 0.0628
• Weighted residual factors for significantly intense reflections: 0.1466
• Weighted residual factors for all reflections included in the refinement: 0.1521
• Goodness-of-fit parameter for all reflections included in the refinement: 1.196
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No