Information card for entry 7236502

Structure parameters

• Formula: C20 H16 F3 N3 O3
• Calculated formula: C20 H16 F3 N3 O3
• Title of publication: Direct C(sp2)‒H amination of aryl aldehyde-derived hydrazones via visible light promoted photoredox catalysis
• Authors of publication: Zhu, Xin; He, Zhi; Li, Qiu-Yan; Wang, Xiao-Jun
• Journal of publication: RSC Advances
• Year of publication: 2017
• Journal volume: 7
• Journal issue: 40
• Pages of publication: 25171
• a: 19.52 ± 0.004 Å
• b: 13.946 ± 0.003 Å
• c: 13.312 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3623.9 ± 1.4 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153.15 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0719
• Residual factor for significantly intense reflections: 0.0669
• Weighted residual factors for significantly intense reflections: 0.1318
• Weighted residual factors for all reflections included in the refinement: 0.1341
• Goodness-of-fit parameter for all reflections included in the refinement: 1.251
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No