Information card for entry 7238390

Structure parameters

• Formula: C64 H64 B N4 Ni2 O8 Rb
• Calculated formula: C64 H64 B N4 Ni2 O8 Rb
• Title of publication: Syntheses, crystal structures and supramolecular topologies of nickel(II)‒s/p/d10/NH4+ complexes derived from a compartmental ligand
• Authors of publication: Sarkar, Sohini; Mohanta, Sasankasekhar
• Journal of publication: RSC Advances
• Year of publication: 2011
• Journal volume: 1
• Journal issue: 4
• Pages of publication: 640
• a: 16.0343 ± 0.0019 Å
• b: 16.0435 ± 0.0019 Å
• c: 25.379 ± 0.003 Å
• α: 83.81 ± 0.002°
• β: 83.857 ± 0.002°
• γ: 68.346 ± 0.002°
• Cell volume: 6016.6 ± 1.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1184
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.0968
• Weighted residual factors for all reflections included in the refinement: 0.113
• Goodness-of-fit parameter for all reflections included in the refinement: 0.901
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No