Information card for entry 7238392

Structure parameters

• Formula: C60 H66 Cl2 Mg N6 Ni3 O24
• Calculated formula: C60 H66 Cl2 Mg N6 Ni3 O24
• Title of publication: Syntheses, crystal structures and supramolecular topologies of nickel(II)‒s/p/d10/NH4+ complexes derived from a compartmental ligand
• Authors of publication: Sarkar, Sohini; Mohanta, Sasankasekhar
• Journal of publication: RSC Advances
• Year of publication: 2011
• Journal volume: 1
• Journal issue: 4
• Pages of publication: 640
• a: 15.4418 ± 0.0013 Å
• b: 22.4552 ± 0.0018 Å
• c: 18.8479 ± 0.0014 Å
• α: 90°
• β: 94.555 ± 0.002°
• γ: 90°
• Cell volume: 6514.8 ± 0.9 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1042
• Residual factor for significantly intense reflections: 0.0512
• Weighted residual factors for significantly intense reflections: 0.1356
• Weighted residual factors for all reflections included in the refinement: 0.1661
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No