Information card for entry 7238394

Structure parameters

• Formula: C22 H25 Cd N5 Ni O10
• Calculated formula: C22 H25 Cd N5 Ni O10
• Title of publication: Syntheses, crystal structures and supramolecular topologies of nickel(II)–s/p/d10/NH4+ complexes derived from a compartmental ligand
• Authors of publication: Sarkar, Sohini; Mohanta, Sasankasekhar
• Journal of publication: RSC Advances
• Year of publication: 2011
• Journal volume: 1
• Journal issue: 4
• Pages of publication: 640
• a: 8.0768 ± 0.0013 Å
• b: 12.074 ± 0.002 Å
• c: 14.348 ± 0.002 Å
• α: 67.471 ± 0.005°
• β: 89.983 ± 0.005°
• γ: 83.029 ± 0.006°
• Cell volume: 1281.2 ± 0.3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1169
• Residual factor for significantly intense reflections: 0.0679
• Weighted residual factors for significantly intense reflections: 0.1724
• Weighted residual factors for all reflections included in the refinement: 0.1968
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No