Information card for entry 7238404

Structure parameters

• Formula: C61.28 H50.56 B2 Cl2.56 F30 K2 O16 S
• Calculated formula: C61.279 H50.558 B2 Cl2.558 F30 K2 O16 S
• Title of publication: Stable sulfate and nitrate borane-adduct anions
• Authors of publication: Becker, Martin; Schulz, Axel; Villinger, Alexander; Voss, Karsten
• Journal of publication: RSC Advances
• Year of publication: 2011
• Journal volume: 1
• Journal issue: 1
• Pages of publication: 128
• a: 14.309 ± 0.005 Å
• b: 22.551 ± 0.009 Å
• c: 24.2 ± 0.008 Å
• α: 102.53 ± 0.03°
• β: 98.78 ± 0.03°
• γ: 100.4 ± 0.03°
• Cell volume: 7347 ± 5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.085
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.1229
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No