Information card for entry 7238478

Structure parameters

• Formula: C20 H32 F3 N3 O11 Os2 S
• Calculated formula: C20 H32 F3 N3 O11 Os2 S
• Title of publication: Synthesis and X-ray diffraction structures of novel half-sandwich Os(ii)-and Ru(ii)-hydroxamate complexes
• Authors of publication: Godó, Attila J.; Bényei, Attila Cs.; Duff, Brian; Egan, Denise A.; Buglyó, Péter
• Journal of publication: RSC Adv.
• Year of publication: 2012
• Journal volume: 2
• Journal issue: 4
• Pages of publication: 1486
• a: 14.2845 ± 0.0003 Å
• b: 9.4565 ± 0.0002 Å
• c: 21.8716 ± 0.0004 Å
• α: 90°
• β: 105.511 ± 0.002°
• γ: 90°
• Cell volume: 2846.84 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0243
• Residual factor for significantly intense reflections: 0.0184
• Weighted residual factors for all reflections included in the refinement: 0.0417
• Goodness-of-fit parameter for all reflections included in the refinement: 0.958
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No