Information card for entry 7238587

Structure parameters

• Formula: C202 H182 Cl8 Cu8 N50 O38
• Calculated formula: C202 H182 Cl8 Cu8 N50 O38
• Title of publication: An octanuclear helical ‘molecular wheel’ from hierarchical assembly of four dinuclear Cu2 units in a mixed-ligand array
• Authors of publication: Najar, Adel M.; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: RSC Advances
• Year of publication: 2012
• Journal volume: 2
• Journal issue: 4
• Pages of publication: 1326
• a: 37.5021 ± 0.0011 Å
• b: 15.4876 ± 0.0004 Å
• c: 42.453 ± 0.0012 Å
• α: 90°
• β: 114.594 ± 0.001°
• γ: 90°
• Cell volume: 22420.5 ± 1.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.1656
• Residual factor for significantly intense reflections: 0.1097
• Weighted residual factors for significantly intense reflections: 0.3292
• Weighted residual factors for all reflections included in the refinement: 0.3609
• Goodness-of-fit parameter for all reflections included in the refinement: 1.187
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No